Test Methods

Below are the Test Methods employed by Fujipoly.

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Test Method of Thermal Conductivity by ISO / CD 22007-2

Fujipoly Test Method: FTM P-1612 (Hot Disk method)

The probe of which the thermal conductivity is known is put on the specimen. Then the hot wire is given constant electric power.

See our video showcase of the FTM P-1612 test method

1. Method

The probe of which the thermal conductivity is known is put on the specimen. Then the hot wire is given constant electric power.

2. Principle

A thermal conductivity is given by the equation below.

3. Apparatus

Thermal Conductivity meter
TPS-2500S
Sensor
RTK Polyimide

Test Methods of Thermal Conductivity by ASTM D2326 equivalent

Fujipoly Test Method: FTM P-1620 (Hot Wire method)

1. Method

The probe of which the thermal conductivity is known is put on the specimen. Then the hot wire is given constant electric power. Thermal conductivity is calculated by software for calculation.

2. Principle

A thermal conductivity is given by the equation below.

3. Apparatus

Thermal Conductivity meter
QTM-D3
Sensor
PC9801BX2
Probe
QTM-PD1

Test Methods of Thermal Resistance by ASTM D5470 equivalent

Fujipoly Test Method: FTM P-3050 (TIM Tester method)

See our video showcase of the FTM P-3050 test method

1. Principle

Thermal Resistance

2. Measuring Equipment

Analysis Tech TIM Tester 1400

The Analysis Tech TIM Tester 1400 automatically includes the overall estimated accuracy with the thermal impedance data. This measuring equipment conforms to the test method ASTM D5470, Thermal Transmission Properties of Thermally Conductive Electrical Insulation Materials with the most recent revision.

Test Method of Thermal Resistance and Thermal Conductivity by ASTM D5470 modified

Fujipoly Test Method: FTM P-3030 (Guarded Hot Plate method)

1. Principles

Thermal Resistance

Thermal Conductivity

Test Method of Thermal Resistance by ASTM D5470 modified by Fujipoly Original

Fujipoly Test Method FTM P-3070

2. Principle

Fujipoly Test Method FTM P-A thermal impedance is given by the equation below: Rt = (Tc - Tf) x S / P0

Rt
: Thermal resistance K-cm2 / W)
Tc
: T1 temperature (K)
Tf
: T2 temperature (K)
S
: Sample Installation Area (cm2)
P0
: Electric Piwer (W)

1. Test Method

FUJIPOLY test method FTM P-3070 which gives ASTM D5470 equivalent value. The sample is sandwiched between aluminum blocks with thermocouples installed, screwed with a specified torque, constant power is applied to the heater to generate constant heat, and the thermal resistance value is measured from the temperature difference between the upper and lower thermocouples.

Test Method of Compression Force by ASTM D575-91

See our video showcase of the Viscosity Measurement Method

1. Test Method

Compression test in which the force required to cause a specified deflection is determined.

2. Test Condition

Specimen
Dia.28.6mm (1.13in)
Thickness is according to each materials
Number of specimens; 3pcs
Platens
Dia.28.6mm (1.13in)
Compression Speed
5.0mm/min (0.2in/min)
*Fujipoly original speed

Test Method of Viscosity by ASTM D1824 – 95(2010) Modified

See our video showcase of the Compression Force test method

1. Test Method

Covers the measurement of SARCON’s viscosity at low shear rates.

2. Apparatus

Equipment
HAAKE MARKS3
Sensor
C20/2
Clearance Gap
0.5mm
Rotational Speed
0.5(1/s), 1.0(1/s)

Fujipoly has been utilizing TIM Tester method and Hot Disk method since Fujipoly defined them as Fujipoly standard.

Current Fujipoly Standard test method

  • Hot Disk method for Thermal Conductivity testing
  • TIM-Tester method for Thermal Resistance testing

Back Ground

  • Hot Wire method was inefficient to test over 4 W/m-K material for Thermal Conductivity due to unstable Contact Thermal Resistance, and it was worse than TO-3 method in 2000.
  • Guarded Heater method was more efficient than TO-3 method, so it was defined as Fujipoly standard method in 2002.
  • After that, Hot Disk method and TIM-Tester method were both defined as latest Fujipoly standard method due to so reliable in 2012.

1. Hot Disk Method for Thermal Conductivity (TC) measuring

  • Advantage: The measured TC does not depend on the specimen’s surface-roughness and hardness due to wide measuring range. And it is more stable than How Wire method.
  • Disadvantage: Specimen’s dimensions, 50 sq-mm x 7mm thickness is so big that the measured TC is a little different from the true one.

2. TIM Tester Method for Thermal Resistance (TR) measuring

  • Advantage: The measured TR can be close to the true TR due each specimen’s thickness.
  • Disadvantage: The measured TR depends on the specimen’s surface-roughness or hardness, and it is not stable.

3. Hot Wire method for TC measuring.

  • Problem: The measured TC is unstable depending on the specimen’s surface-roughness due to fixed-point type thermocouple.

4. Guarded Heater method modified ASTM D 5470 for TR measuring.

  • Problem: The measured TR is lower than the true one because it is impossible to prevent heat dissipation from the Aluminum blocks which hold the specimen. It is also unstable under continuous compression depending on specimen’s deformation which comes from small difference in hardness and modulus.

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